Table 4. Precision, recovery and accuracy of the analyses of the target barbiturates in raw milk

Compound Concentration(ng/g milk) Replicate number Recovery (%) Intra-day RSD (%) Intra-day RSD (%) Accuracy (%)
Phenobarbital 10 6 86.4-100.0 1.4-5.6 3.9 94.6-117.2
20 6 85.8-111.4 2.5-8.5 6.0 92.2-127.0
40 6 85.0-110.6 3.8-9.8 7.3 88.5-118.8